Pesticide residues in sauce manufactured from agricultural products

Tarık Balkan; Kenan Kara

Article Details

Pesticide residues in sauce manufactured from agricultural products

Authors:

Tarık Balkan | Kenan Kara

Publisher:

Gültekin ÖZDEMİR

Main Topics:

Agricultural Engineering (Other)

Journal:

International Journal of Agriculture Environment and Food Sciences Vol.7 Issue 1, pp.131-135

Document Type:

Article

Publication Date:

3/2023

Document Language:

English

Document ID (Org No.):

2001282204

pISSN:

2618-5946

Keywords:

Abstract:

 In this study, pesticide residues in sauce manufactured from agricultural products were examined. A simultaneous multiresidue analysis for 260 pesticides in sauce samples was performed using liquid chromatography with tandem mass spectrometry LC-MSMS. The QuEChERS AOAC 2007.01 quick, easy, cheap, effective, rugged, and safe was selected as the most suitable protocol for routine determination of pesticide residues. In line with the SANTE113122021 guideline two parameters were used as identification criteria: retention time RT with a tolerance of  0.1 min in relation to the RT of the analyte in matrix-matched calibration standard and ion ratio tolerance below 30. The RT deviation in positive samples was always  0.1 min, and the ion ratio tolerance was  30. A total 4 different pesticides were detected in 20 sauce samples. No active ingredient was found in 16 samples. The residue levels were between 10 and 94 µg kg. The residues of acetamiprid, ametoctradin, imazalil sulfate, and metalaxyl-M were below the European Union Maximum Residue Limits EU-MRLs.

 In this study, pesticide residues in sauce manufactured from agricultural products were examined. A simultaneous multiresidue analysis for 260 pesticides in sauce samples was performed using liquid chromatography with tandem mass spectrometry LC-MSMS. The QuEChERS AOAC 2007.01 quick, easy, cheap, effective, rugged, and safe was selected as the most suitable protocol for routine determination of pesticide residues. In line with the SANTE113122021 guideline two parameters were used as identification criteria: retention time RT with a tolerance of  0.1 min in relation to the RT of the analyte in matrix-matched calibration standard and ion ratio tolerance below 30. The RT deviation in positive samples was always  0.1 min, and the ion ratio tolerance was  30. A total 4 different pesticides were detected in 20 sauce samples. No active ingredient was found in 16 samples. The residue levels were between 10 and 94 µg kg. The residues of acetamiprid, ametoctradin, imazalil sulfate, and metalaxyl-M were below the European Union Maximum Residue Limits EU-MRLs.

 In this study, pesticide residues in sauce manufactured from agricultural products were examined. A simultaneous multiresidue analysis for 260 pesticides in sauce samples was performed using liquid chromatography with tandem mass spectrometry LC-MSMS. The QuEChERS AOAC 2007.01 quick, easy, cheap, effective, rugged, and safe was selected as the most suitable protocol for routine determination of pesticide residues. In line with the SANTE113122021 guideline two parameters were used as identification criteria: retention time RT with a tolerance of  0.1 min in relation to the RT of the analyte in matrix-matched calibration standard and ion ratio tolerance below 30. The RT deviation in positive samples was always  0.1 min, and the ion ratio tolerance was  30. A total 4 different pesticides were detected in 20 sauce samples. No active ingredient was found in 16 samples. The residue levels were between 10 and 94 µg kg. The residues of acetamiprid, ametoctradin, imazalil sulfate, and metalaxyl-M were below the European Union Maximum Residue Limits EU-MRLs.

 In this study, pesticide residues in sauce manufactured from agricultural products were examined. A simultaneous multiresidue analysis for 260 pesticides in sauce samples was performed using liquid chromatography with tandem mass spectrometry LC-MSMS. The QuEChERS AOAC 2007.01 quick, easy, cheap, effective, rugged, and safe was selected as the most suitable protocol for routine determination of pesticide residues. In line with the SANTE113122021 guideline two parameters were used as identification criteria: retention time RT with a tolerance of  0.1 min in relation to the RT of the analyte in matrix-matched calibration standard and ion ratio tolerance below 30. The RT deviation in positive samples was always  0.1 min, and the ion ratio tolerance was  30. A total 4 different pesticides were detected in 20 sauce samples. No active ingredient was found in 16 samples. The residue levels were between 10 and 94 µg kg. The residues of acetamiprid, ametoctradin, imazalil sulfate, and metalaxyl-M were below the European Union Maximum Residue Limits EU-MRLs.

Article Details

Pesticide residues in sauce manufactured from agricultural products

Authors:

Tarık Balkan | Kenan Kara

Publisher:

Gültekin ÖZDEMİR

Main Topics:

Agricultural Engineering (Other)

Journal:

International Journal of Agriculture Environment and Food Sciences Vol.7 Issue 1, pp.131-135

Document Type:

Article

Publication Date:

3/2023

Document Language:

English

Document ID (Org No.):

2001282204

pISSN:

2618-5946

Pesticide residue

Processing factor

Sauce

Tomato

LC-MS/MS

QuEChERS

Pesticide residue

Processing factor

Sauce

Tomato

LC-MS/MS

Pesticide residue

Processing factor

Sauce

Tomato

LC-MS/MS

QuEChERS

Issues

Article Details

Authors: Tarık Balkan | Kenan Kara

Publisher: Gültekin ÖZDEMİR

Main Topics: Agricultural Engineering (Other)

Journal: International Journal of Agriculture Environment and Food Sciences Vol.7 Issue 1, pp.131-135

Document Type: Article

Publication Date: 3/2023

Document Language: English

Document ID (Org No.): 2001282204

pISSN: 2618-5946

Issues

Authors:

Tarık Balkan | Kenan Kara

Publisher:

Gültekin ÖZDEMİR

Main Topics:

Agricultural Engineering (Other)

Journal:

International Journal of Agriculture Environment and Food Sciences Vol.7 Issue 1, pp.131-135

Document Type:

Article

Publication Date:

3/2023

Document Language:

English

Document ID (Org No.):

2001282204

pISSN:

2618-5946