Fe3O4@SA MNCs Synthesis, Characterization, and First-time Use in Hydrogen Production by NaBH4 Hydrolysis

Adil Umaz

Article Details

Fe3O4@SA MNCs Synthesis, Characterization, and First-time Use in Hydrogen Production by NaBH4 Hydrolysis

Authors:

Adil Umaz

Publisher:

Turkish Chemical Society

Main Topics:

Analytical Chemistry (Other)

Journal:

Journal of the Turkish Chemical Society Section A: Chemistry Vol.11 Issue 1, pp.205-216

Document Type:

Article

Publication Date:

4/2024

Document Language:

English

Document ID (Org No.):

2001303743

pISSN:

2149-0120

Keywords:

Abstract:

 Hydrogen is a clean energy carrier that will reduce dependence on fossil fuels and contribute to reducing the harmful effects on the environment resulting from using fossil fuels. Hydrogen is produced by the hydrolysis of sodium borohydride NaBH4, one of the chemical hydrides, using a catalyst. In this study, Fe3O4Salicylic acid magnetic nano-catalyst Fe3O4SA MNCs was synthesized using the co-precipitation technique. The structural, physical, and chemical properties of the produced Fe3O4SA MNCs were characterized by FT-IR, XRD, VSM, SEM, and SEM-EDX methods. At room temperature, the effect on hydrogen production performance was examined in the amounts of Fe3O4SA MNCs 10, 25, 50, 75, and 100 mg, NaOH 0, 10, 20, and 25 mg, and NaBH4 25, 50, 100, 150 and 200 mg. The highest hydrogen generation rates HGR were obtained using 10 mg Fe3O4SA MNCs, 150 mg NaBH4, and 0 mg NaOH at room temperature. The obtained HGR value was calculated as 400 mL gcat-1.min-1. Fe3O4SA MNCs were used for hydrogen production for the first time in this study. This study showed that Fe3O4SA MNCs exhibit catalytic properties and are a promising, efficient catalyst in hydrogen production from NaBH4.

 Hydrogen is a clean energy carrier that will reduce dependence on fossil fuels and contribute to reducing the harmful effects on the environment resulting from using fossil fuels. Hydrogen is produced by the hydrolysis of sodium borohydride NaBH4, one of the chemical hydrides, using a catalyst. In this study, Fe3O4Salicylic acid magnetic nano-catalyst Fe3O4SA MNCs was synthesized using the co-precipitation technique. The structural, physical, and chemical properties of the produced Fe3O4SA MNCs were characterized by FT-IR, XRD, VSM, SEM, and SEM-EDX methods. At room temperature, the effect on hydrogen production performance was examined in the amounts of Fe3O4SA MNCs 10, 25, 50, 75, and 100 mg, NaOH 0, 10, 20, and 25 mg, and NaBH4 25, 50, 100, 150 and 200 mg. The highest hydrogen generation rates HGR were obtained using 10 mg Fe3O4SA MNCs, 150 mg NaBH4, and 0 mg NaOH at room temperature. The obtained HGR value was calculated as 400 mL gcat-1.min-1. Fe3O4SA MNCs were used for hydrogen production for the first time in this study. This study showed that Fe3O4SA MNCs exhibit catalytic properties and are a promising, efficient catalyst in hydrogen production from NaBH4.

 Hydrogen is a clean energy carrier that will reduce dependence on fossil fuels and contribute to reducing the harmful effects on the environment resulting from using fossil fuels. Hydrogen is produced by the hydrolysis of sodium borohydride NaBH4, one of the chemical hydrides, using a catalyst. In this study, Fe3O4Salicylic acid magnetic nano-catalyst Fe3O4SA MNCs was synthesized using the co-precipitation technique. The structural, physical, and chemical properties of the produced Fe3O4SA MNCs were characterized by FT-IR, XRD, VSM, SEM, and SEM-EDX methods. At room temperature, the effect on hydrogen production performance was examined in the amounts of Fe3O4SA MNCs 10, 25, 50, 75, and 100 mg, NaOH 0, 10, 20, and 25 mg, and NaBH4 25, 50, 100, 150 and 200 mg. The highest hydrogen generation rates HGR were obtained using 10 mg Fe3O4SA MNCs, 150 mg NaBH4, and 0 mg NaOH at room temperature. The obtained HGR value was calculated as 400 mL gcat-1.min-1. Fe3O4SA MNCs were used for hydrogen production for the first time in this study. This study showed that Fe3O4SA MNCs exhibit catalytic properties and are a promising, efficient catalyst in hydrogen production from NaBH4.

 Hydrogen is a clean energy carrier that will reduce dependence on fossil fuels and contribute to reducing the harmful effects on the environment resulting from using fossil fuels. Hydrogen is produced by the hydrolysis of sodium borohydride NaBH4, one of the chemical hydrides, using a catalyst. In this study, Fe3O4Salicylic acid magnetic nano-catalyst Fe3O4SA MNCs was synthesized using the co-precipitation technique. The structural, physical, and chemical properties of the produced Fe3O4SA MNCs were characterized by FT-IR, XRD, VSM, SEM, and SEM-EDX methods. At room temperature, the effect on hydrogen production performance was examined in the amounts of Fe3O4SA MNCs 10, 25, 50, 75, and 100 mg, NaOH 0, 10, 20, and 25 mg, and NaBH4 25, 50, 100, 150 and 200 mg. The highest hydrogen generation rates HGR were obtained using 10 mg Fe3O4SA MNCs, 150 mg NaBH4, and 0 mg NaOH at room temperature. The obtained HGR value was calculated as 400 mL gcat-1.min-1. Fe3O4SA MNCs were used for hydrogen production for the first time in this study. This study showed that Fe3O4SA MNCs exhibit catalytic properties and are a promising, efficient catalyst in hydrogen production from NaBH4.

Article Details

Fe3O4@SA MNCs Synthesis, Characterization, and First-time Use in Hydrogen Production by NaBH4 Hydrolysis

Authors: Adil Umaz

Publisher: Turkish Chemical Society

Main Topics: Analytical Chemistry (Other)

Journal: Journal of the Turkish Chemical Society Section A: Chemistry Vol.11 Issue 1, pp.205-216

Document Type: Article

Publication Date: 4/2024

Document Language: English

Document ID (Org No.): 2001303743

pISSN: 2149-0120

Fe3O4@SA

hydrogen production

magnetic nano-catalyst

NaBH4

Issues

Authors:

Adil Umaz

Publisher:

Turkish Chemical Society

Main Topics:

Analytical Chemistry (Other)

Journal:

Journal of the Turkish Chemical Society Section A: Chemistry Vol.11 Issue 1, pp.205-216

Document Type:

Article

Publication Date:

4/2024

Document Language:

English

Document ID (Org No.):

2001303743

pISSN:

2149-0120