Synthesis and characterization of some new2- mercapto benzimidazole derivative from ortho phenylenediamine

Ihmood Kh .jebur; Noaman F.N. Al-hitti

Article Details

Synthesis and characterization of some new2- mercapto benzimidazole derivative from ortho phenylenediamine

Authors:

Ihmood Kh .jebur | Noaman F.N. Al-hitti

Publisher:

University of Kirkuk

Journal:

Kirkuk Journal of Science Vol.10 Issue 4, pp.222-239

Document Type:

Article

Publication Date:

12/2015

Document Language:

English

Document ID (Org No.):

2001931779

pISSN:

3005-4788

Keywords:

Abstract:

 of hydrazones (N3- N10) were synthesized from the reaction of compound (N2) with various substituted  benzaldehydes (aceto phenone) gave hydrazone compounds(N3-N10).Substituted compounds(N11-N12) , compound (N13) , compounds(N14-N16) ,compounds (N17-N18),Were synthesized from cyclization of hydrazones (N3- N10) using chloro acetic acid or tri chloro acetic acid or thio glycolic acid or chloro acetyl chloride respectively.
The synthesized compounds were identified according to their physical properties, spectroscopic data (IR and1H- NMR) in addition to systematic identification of some active functional groups in these compounds. This the research includes synthesis of some new derivatives of 2-mercapto benzimidazole (N1), the compound (N1), prepared by reaction of o-phenylene  diamine with carbon disulfide in alcoholic potassium hydroxide. Then the compound (N1) was treated with hydrazine hydrate in ethanol to give 2-hydrazinobenzimidazole ( N2).A Number.

Article Details

Synthesis and characterization of some new2- mercapto benzimidazole derivative from ortho phenylenediamine

Authors:

Ihmood Kh .jebur | Noaman F.N. Al-hitti

Publisher:

University of Kirkuk

Journal:

Kirkuk Journal of Science Vol.10 Issue 4, pp.222-239

Document Type:

Article

Publication Date:

12/2015

Document Language:

English

Document ID (Org No.):

2001931779

pISSN:

3005-4788

Mercaptobenzimidazole

benzimidazole

Oxazolidine

One

Issues

Article Details

Synthesis and characterization of some new2- mercapto benzimidazole derivative from ortho phenylenediamine

Authors: Ihmood Kh .jebur | Noaman F.N. Al-hitti

Publisher: University of Kirkuk

Journal: Kirkuk Journal of Science Vol.10 Issue 4, pp.222-239

Document Type: Article

Publication Date: 12/2015

Document Language: English

Document ID (Org No.): 2001931779

pISSN: 3005-4788

Mercaptobenzimidazole

benzimidazole

Oxazolidine

One

Issues

Authors:

Ihmood Kh .jebur | Noaman F.N. Al-hitti

Publisher:

University of Kirkuk

Journal:

Kirkuk Journal of Science Vol.10 Issue 4, pp.222-239

Document Type:

Article

Publication Date:

12/2015

Document Language:

English

Document ID (Org No.):

2001931779

pISSN:

3005-4788