Extraction and Characterization of Linden Tree Seed Oil Grown in Malatya with Different Solvents

Yunus Önal; Tuğçe Begüm Mumcu; Tuğba Utku

Article Details

Extraction and Characterization of Linden Tree Seed Oil Grown in Malatya with Different Solvents

Authors:

Yunus Önal | Tuğçe Begüm Mumcu | Tuğba Utku

Publisher:

Van Yuzuncu Yıl University

Main Topics:

Mühendislik

Journal:

Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.28 Issue 3, pp.857-870

Document Type:

Article

Publication Date:

12/2023

Document Language:

English

Document ID (Org No.):

2001307798

pISSN:

1300-5413

Keywords:

Abstract:

 In this study, the characterization study of the oil of linden seeds obtained by the extraction method was carried out. The outer shells of linden seeds collected from Malatya region in August 2018 were cleaned before extraction. Hexane, ethyl alcohol and acetone were used as solvents. Elemental analysis, XRD X-Ray Diffraction, SEM Scanning Electron Microscopy, ash determination and saponification number determinations were performed for characterization processes. After the analysis, the oil yield with ethyl alcohol was determined as 33 by weight with acetone, 28.65 for hexane and 28 for acetone. In linden seed fatty acid, it was determined as oleic acid: 27.442 for acetone, 30.852 for hexane, 10.955 for acetone by weight, 11.929 for hexane, linoleic acid: 51.188 for acetone, 44.145 for hexane. The soap number value was determined as 232.48 mg KOHg for ethyl alcohol, 176.72 mgKOHg for hexane and 246.94 mg KOHg oil for acetone. While the ash determination value was 5.755 for the seed, the shell ash was determined as 2.1 differently.

 In this study, the characterization study of the oil of linden seeds obtained by the extraction method was carried out. The outer shells of linden seeds collected from Malatya region in August 2018 were cleaned before extraction. Hexane, ethyl alcohol and acetone were used as solvents. Elemental analysis, XRD X-Ray Diffraction, SEM Scanning Electron Microscopy, ash determination and saponification number determinations were performed for characterization processes. After the analysis, the oil yield with ethyl alcohol was determined as 33 by weight with acetone, 28.65 for hexane and 28 for acetone. In linden seed fatty acid, it was determined as oleic acid: 27.442 for acetone, 30.852 for hexane, 10.955 for acetone by weight, 11.929 for hexane, linoleic acid: 51.188 for acetone, 44.145 for hexane. The soap number value was determined as 232.48 mg KOHg for ethyl alcohol, 176.72 mgKOHg for hexane and 246.94 mg KOHg oil for acetone. While the ash determination value was 5.755 for the seed, the shell ash was determined as 2.1 differently.

 In this study, the characterization study of the oil of linden seeds obtained by the extraction method was carried out. The outer shells of linden seeds collected from Malatya region in August 2018 were cleaned before extraction. Hexane, ethyl alcohol and acetone were used as solvents. Elemental analysis, XRD X-Ray Diffraction, SEM Scanning Electron Microscopy, ash determination and saponification number determinations were performed for characterization processes. After the analysis, the oil yield with ethyl alcohol was determined as 33 by weight with acetone, 28.65 for hexane and 28 for acetone. In linden seed fatty acid, it was determined as oleic acid: 27.442 for acetone, 30.852 for hexane, 10.955 for acetone by weight, 11.929 for hexane, linoleic acid: 51.188 for acetone, 44.145 for hexane. The soap number value was determined as 232.48 mg KOHg for ethyl alcohol, 176.72 mgKOHg for hexane and 246.94 mg KOHg oil for acetone. While the ash determination value was 5.755 for the seed, the shell ash was determined as 2.1 differently.

 Bu çalışmada Ekstraksiyon metodu ile elde edilen Ihlamur tohumlarının yağının karakterizasyon çalışması yapıldı. 2018 yılının Ağustos ayında Malatya yöresinden toplanan ıhlamur tohumlarının dış kabukları ekstraksiyon öncesi temizlendi. Çözücü olarak hekzan, etil alkol ve aseton kullanıldı. Karakterizasyon işlemleri için element analizi, XRD X-Işınları Difraksiyonu, SEM Taramalı Elektron Mikroskobu, kül tayini ve sabunlaşma sayısı tayinleri yapıldı. Analiz sonrası etil alkol ile yağ verimi ağırlıkça aseton ile yağ verimi  33, hekzan için 28.65 ve asoton için yağ verimi  28 olarak tayin edildi. Ihlamur tohumu yağ asidinde ağırlıkça oleik asit: aseton için 27.442, hekzan için 30.852, ağırlıkça palmitik asit: aseton için 10.955, hekzan için 11.929, ağırlıkça linoleik asit: aseton için 51.188, hekzan için 44.145 olarak tayin edildi. Sabun sayısı değeri ise etil alkol için 232.48 mg KOHg, hekzan için 176.72 mgKOHg ve aseton için 246.94 mg KOHg yağ olarak tayin edildi. Kül tayini değeri tohum için 5.575 iken kabuk külü farklı olarak 2.1 olarak tayin edildi.

Article Details

Extraction and Characterization of Linden Tree Seed Oil Grown in Malatya with Different Solvents

Authors:

Yunus Önal | Tuğçe Begüm Mumcu | Tuğba Utku

Publisher:

Van Yuzuncu Yıl University

Main Topics:

Mühendislik

Journal:

Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.28 Issue 3, pp.857-870

Document Type:

Article

Publication Date:

12/2023

Document Language:

English

Document ID (Org No.):

2001307798

pISSN:

1300-5413

Fatty acids

Linden seed

Solvent

SoxhletÇözgen

Ihlamur tohumu

Sokslet

Yağ asitleri

Issues

Article Details

Authors: Yunus Önal | Tuğçe Begüm Mumcu | Tuğba Utku

Publisher: Van Yuzuncu Yıl University

Main Topics: Mühendislik

Journal: Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.28 Issue 3, pp.857-870

Document Type: Article

Publication Date: 12/2023

Document Language: English

Document ID (Org No.): 2001307798

pISSN: 1300-5413

Issues

Authors:

Yunus Önal | Tuğçe Begüm Mumcu | Tuğba Utku

Publisher:

Van Yuzuncu Yıl University

Main Topics:

Mühendislik

Journal:

Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi Vol.28 Issue 3, pp.857-870

Document Type:

Article

Publication Date:

12/2023

Document Language:

English

Document ID (Org No.):

2001307798

pISSN:

1300-5413