Green synthesis of Fe3O4 nanoparticles by one-pot  saccharide-assisted hydrothermal method

Ayşe DEMİR; Abdulhadi BAYKAL; Hüseyin SÖZERİ

Article Details

Green synthesis of Fe3O4 nanoparticles by one-pot saccharide-assisted hydrothermal method

Authors:

Ayşe DEMİR | Abdulhadi BAYKAL | Hüseyin SÖZERİ

Publisher:

TUBITAK

Journal:

Turkish Journal of Chemistry 2014 Vol.38 Issue 5, pp.825-836

Document Type:

Article

Publication Date:

4/2014

Document Language:

Turkish

Document ID (Org No.):

2000727088

Frequency:

Bimonthly

eISSN:

1303-6130

pISSN:

1300-0527

Abstract:

 

A saccharide-assisted hydrothermal route starting from a  single iron precursor was employed to study the influence of reducing  saccharides on the formation of iron oxide (Fe3O4) nanoparticles  (NPs). Fe3O4 NPs, which were confirmed by X-ray diffraction  analysis, were successfully synthesized by a hydrothermal method in which  mannose, maltose, lactose, and galactose served as reducing agents. The  formation of Fe3O4 NPs was also confirmed by Fourier transform  infrared spectroscopy. Samples exhibited different crystallite sizes  estimated based on line profile fitting as 12 \pm  2, 9 \pm  2, 13 \pm   3, and 9 \pm  3 nm for mannose, maltose, lactose, and galactose,  respectively. Magnetic characterization results revealed superparamagnetic  features of the NPs obtained with galactose, mannose, and maltose.

 

A saccharide-assisted hydrothermal route starting from a  single iron precursor was employed to study the influence of reducing  saccharides on the formation of iron oxide (Fe3O4) nanoparticles  (NPs). Fe3O4 NPs, which were confirmed by X-ray diffraction  analysis, were successfully synthesized by a hydrothermal method in which  mannose, maltose, lactose, and galactose served as reducing agents. The  formation of Fe3O4 NPs was also confirmed by Fourier transform  infrared spectroscopy. Samples exhibited different crystallite sizes  estimated based on line profile fitting as 12 \pm  2, 9 \pm  2, 13 \pm   3, and 9 \pm  3 nm for mannose, maltose, lactose, and galactose,  respectively. Magnetic characterization results revealed superparamagnetic  features of the NPs obtained with galactose, mannose, and maltose.

Article Details

Green synthesis of Fe3O4 nanoparticles by one-pot saccharide-assisted hydrothermal method

Authors: Ayşe DEMİR | Abdulhadi BAYKAL | Hüseyin SÖZERİ

Publisher: TUBITAK

Journal: Turkish Journal of Chemistry 2014 Vol.38 Issue 5, pp.825-836

Document Type: Article

Publication Date: 4/2014

Document Language: Turkish

Document ID (Org No.): 2000727088

Frequency: Bimonthly

eISSN: 1303-6130

pISSN: 1300-0527

Issues

Authors:

Ayşe DEMİR | Abdulhadi BAYKAL | Hüseyin SÖZERİ

Publisher:

TUBITAK

Journal:

Turkish Journal of Chemistry 2014 Vol.38 Issue 5, pp.825-836

Document Type:

Article

Publication Date:

4/2014

Document Language:

Turkish

Document ID (Org No.):

2000727088

Frequency:

Bimonthly

eISSN:

1303-6130

pISSN:

1300-0527